Using Compliant Interlayers as Crack Arresters in 3-D-Printed Polymeric Structures

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Using Compliant Interlayers as Crack Arresters in 3-D-Printed Polymeric Structures. / Arbeiter, Florian; Petersmann, Sandra; Wiener, Johannes et al.
In: Materials Performance and Characterization, Vol. 9, No. 5, 01.11.2020.

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@article{5eef14824fdd44919701fd5b93b9a0cd,
title = "Using Compliant Interlayers as Crack Arresters in 3-D-Printed Polymeric Structures",
abstract = "The aim of this study is to show the influence of using compliant interlayers as crack arresters for three-dimensional (3-D)-printed polymeric structures. To investigate the effectiveness of compliant interlayers, specimens consisting of a stiff and brittle matrix and thin compliant interlayers were printed. The results of these polymeric composites were compared to pure matrix material samples. To generate specimens, a commercially available material extrusion-based desktop 3-Dprinter was used. Additively manufactured samples were tested in both impact as well as fracture mechanical tests. The application of a compliant interlayer as crack arrester showed high potential in both types of test. Instrumented Charpy impact tests according to EN ISO 179-2 revealed an increase of notched impact strength from 5.0 ± 0.1 kJm−2 to 25 kJm−2 (energy up to Fmax) and 136 ± 2.6 kJm−2 (total energy during testing), respectively. This indicates an increase of roughly 725% and 2,720%, while the maximum force during testing remained almost unchanged at approximately 200 N. Interestingly, the exact position as well as the number of compliant interlayers did not show a significant influence on the results. Therefore, tests that are more detailed were conducted on specimens including only a single interlayer. Further tests consisted of J-integral testing on specimens with aforementioned single compliant interlayers. Crack resistance (J-R curves) were generated using the multi-specimen approach and evaluation according to the protocol of the European Structural Integrity Society. Although a special data-shifting procedure has to be applied to interpret results more clearly, J-integral values showed a significant increase of 250 % at the interface between materials compared to the pure matrix material.",
keywords = "Additive manufacturing, Fracture toughness, Fused filament fabrication, Impact testing, Polyethylene terephthalate glycol, Thermoplastic copolyester, Three-dimensional printing",
author = "Florian Arbeiter and Sandra Petersmann and Johannes Wiener and Florian Oesterreicher and Martin Sp{\"o}rk and Pinter, {Gerald Gerhard}",
year = "2020",
month = nov,
day = "1",
doi = "doi:10.1520/MPC20190201",
language = "English",
volume = "9",
journal = "Materials Performance and Characterization",
issn = "2165-3992",
publisher = "ASTM International",
number = "5",

}

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TY - JOUR

T1 - Using Compliant Interlayers as Crack Arresters in 3-D-Printed Polymeric Structures

AU - Arbeiter, Florian

AU - Petersmann, Sandra

AU - Wiener, Johannes

AU - Oesterreicher, Florian

AU - Spörk, Martin

AU - Pinter, Gerald Gerhard

PY - 2020/11/1

Y1 - 2020/11/1

N2 - The aim of this study is to show the influence of using compliant interlayers as crack arresters for three-dimensional (3-D)-printed polymeric structures. To investigate the effectiveness of compliant interlayers, specimens consisting of a stiff and brittle matrix and thin compliant interlayers were printed. The results of these polymeric composites were compared to pure matrix material samples. To generate specimens, a commercially available material extrusion-based desktop 3-Dprinter was used. Additively manufactured samples were tested in both impact as well as fracture mechanical tests. The application of a compliant interlayer as crack arrester showed high potential in both types of test. Instrumented Charpy impact tests according to EN ISO 179-2 revealed an increase of notched impact strength from 5.0 ± 0.1 kJm−2 to 25 kJm−2 (energy up to Fmax) and 136 ± 2.6 kJm−2 (total energy during testing), respectively. This indicates an increase of roughly 725% and 2,720%, while the maximum force during testing remained almost unchanged at approximately 200 N. Interestingly, the exact position as well as the number of compliant interlayers did not show a significant influence on the results. Therefore, tests that are more detailed were conducted on specimens including only a single interlayer. Further tests consisted of J-integral testing on specimens with aforementioned single compliant interlayers. Crack resistance (J-R curves) were generated using the multi-specimen approach and evaluation according to the protocol of the European Structural Integrity Society. Although a special data-shifting procedure has to be applied to interpret results more clearly, J-integral values showed a significant increase of 250 % at the interface between materials compared to the pure matrix material.

AB - The aim of this study is to show the influence of using compliant interlayers as crack arresters for three-dimensional (3-D)-printed polymeric structures. To investigate the effectiveness of compliant interlayers, specimens consisting of a stiff and brittle matrix and thin compliant interlayers were printed. The results of these polymeric composites were compared to pure matrix material samples. To generate specimens, a commercially available material extrusion-based desktop 3-Dprinter was used. Additively manufactured samples were tested in both impact as well as fracture mechanical tests. The application of a compliant interlayer as crack arrester showed high potential in both types of test. Instrumented Charpy impact tests according to EN ISO 179-2 revealed an increase of notched impact strength from 5.0 ± 0.1 kJm−2 to 25 kJm−2 (energy up to Fmax) and 136 ± 2.6 kJm−2 (total energy during testing), respectively. This indicates an increase of roughly 725% and 2,720%, while the maximum force during testing remained almost unchanged at approximately 200 N. Interestingly, the exact position as well as the number of compliant interlayers did not show a significant influence on the results. Therefore, tests that are more detailed were conducted on specimens including only a single interlayer. Further tests consisted of J-integral testing on specimens with aforementioned single compliant interlayers. Crack resistance (J-R curves) were generated using the multi-specimen approach and evaluation according to the protocol of the European Structural Integrity Society. Although a special data-shifting procedure has to be applied to interpret results more clearly, J-integral values showed a significant increase of 250 % at the interface between materials compared to the pure matrix material.

KW - Additive manufacturing

KW - Fracture toughness

KW - Fused filament fabrication

KW - Impact testing

KW - Polyethylene terephthalate glycol

KW - Thermoplastic copolyester

KW - Three-dimensional printing

UR - http://www.scopus.com/inward/record.url?scp=85095568608&partnerID=8YFLogxK

U2 - doi:10.1520/MPC20190201

DO - doi:10.1520/MPC20190201

M3 - Article

VL - 9

JO - Materials Performance and Characterization

JF - Materials Performance and Characterization

SN - 2165-3992

IS - 5

ER -