Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3

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Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3. / Uršič, Hana; Benčan, Andreja; Dražić, Goran et al.
In: Journal of Materials Chemistry B, Vol. 3.2015, No. 39, 09.09.2015, p. 10309-10315.

Research output: Contribution to journal › Article › Research › peer-review

Harvard

Uršič, H, Benčan, A, Dražić, G, Esteves, G, Jones, JL, Usher, T-M, Rojac, T, Drnovšek, S, Deluca, M, Jouin, J, Bobnar, V, Trefalt, G, Holc, J & Malič, B 2015, 'Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3', Journal of Materials Chemistry B, vol. 3.2015, no. 39, pp. 10309-10315. https://doi.org/10.1039/c5tc02205c

APA

Uršič, H., Benčan, A., Dražić, G., Esteves, G., Jones, J. L., Usher, T.-M., Rojac, T., Drnovšek, S., Deluca, M., Jouin, J., Bobnar, V., Trefalt, G., Holc, J., & Malič, B. (2015). Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3. Journal of Materials Chemistry B, 3.2015(39), 10309-10315. https://doi.org/10.1039/c5tc02205c

Vancouver

Uršič H, Benčan A, Dražić G, Esteves G, Jones JL, Usher TM et al. Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3. Journal of Materials Chemistry B. 2015 Sept 9;3.2015(39):10309-10315. doi: 10.1039/c5tc02205c

Author

Uršič, Hana ; Benčan, Andreja ; Dražić, Goran et al. / Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3. In: Journal of Materials Chemistry B. 2015 ; Vol. 3.2015, No. 39. pp. 10309-10315.

Bibtex - Download

@article{b279cb0624c74800a82fbcea581abd41,
title = "Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3",
abstract = "This study demonstrates the important effect of processing on the B-site ordering in Pb(Sc0.5Nb0.5)O3 ceramics. In contradiction to previous observations on ceramics prepared from solid state synthesis powders, which show a distinctive B-site cation ordering when annealed below ∼1200 °C, in mechanochemically derived ceramics sintered 200 °C below this temperature, we do not observe such ordering, regardless of the conditions of thermal post-annealing. Accordingly, atomic-scale transmission electron microscopy revealed nanometer-sized B-site ordered regions in mechanochemically derived ceramics contrary to the larger regions extending through the whole grains in solid-state derived ceramics.",
author = "Hana Ur{\v s}i{\v c} and Andreja Ben{\v c}an and Goran Dra{\v z}i{\'c} and Giovanni Esteves and Jones, {Jacob L.} and Tedi-Marie Usher and Tadej Rojac and Silvo Drnov{\v s}ek and Marco Deluca and Jenny Jouin and Vid Bobnar and Gregor Trefalt and Janez Holc and Barbara Mali{\v c}",
year = "2015",
month = sep,
day = "9",
doi = "10.1039/c5tc02205c",
language = "English",
volume = "3.2015",
pages = "10309--10315",
journal = "Journal of Materials Chemistry B",
issn = "2050-7518",
publisher = "Royal Society of Chemistry",
number = "39",

}

RIS (suitable for import to EndNote) - Download

TY - JOUR

T1 - Unusual structural-disorder stability of mechanochemically derived-Pb(Sc0.5Nb0.5)O3

AU - Uršič, Hana

AU - Benčan, Andreja

AU - Dražić, Goran

AU - Esteves, Giovanni

AU - Jones, Jacob L.

AU - Usher, Tedi-Marie

AU - Rojac, Tadej

AU - Drnovšek, Silvo

AU - Deluca, Marco

AU - Jouin, Jenny

AU - Bobnar, Vid

AU - Trefalt, Gregor

AU - Holc, Janez

AU - Malič, Barbara

PY - 2015/9/9

Y1 - 2015/9/9

N2 - This study demonstrates the important effect of processing on the B-site ordering in Pb(Sc0.5Nb0.5)O3 ceramics. In contradiction to previous observations on ceramics prepared from solid state synthesis powders, which show a distinctive B-site cation ordering when annealed below ∼1200 °C, in mechanochemically derived ceramics sintered 200 °C below this temperature, we do not observe such ordering, regardless of the conditions of thermal post-annealing. Accordingly, atomic-scale transmission electron microscopy revealed nanometer-sized B-site ordered regions in mechanochemically derived ceramics contrary to the larger regions extending through the whole grains in solid-state derived ceramics.

AB - This study demonstrates the important effect of processing on the B-site ordering in Pb(Sc0.5Nb0.5)O3 ceramics. In contradiction to previous observations on ceramics prepared from solid state synthesis powders, which show a distinctive B-site cation ordering when annealed below ∼1200 °C, in mechanochemically derived ceramics sintered 200 °C below this temperature, we do not observe such ordering, regardless of the conditions of thermal post-annealing. Accordingly, atomic-scale transmission electron microscopy revealed nanometer-sized B-site ordered regions in mechanochemically derived ceramics contrary to the larger regions extending through the whole grains in solid-state derived ceramics.

U2 - 10.1039/c5tc02205c

DO - 10.1039/c5tc02205c

M3 - Article

VL - 3.2015

SP - 10309

EP - 10315

JO - Journal of Materials Chemistry B

JF - Journal of Materials Chemistry B

SN - 2050-7518

IS - 39

ER -

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