Revealing the embrittlement phenomena after post-weld heat treatment of high-strength weld metal using high-resolution microscopy

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Revealing the embrittlement phenomena after post-weld heat treatment of high-strength weld metal using high-resolution microscopy. / Schrittwieser, Daniel; Pahr, Hannes; Musi, Michael et al.
In: Journal of Materials Research and Technology, Vol. 33.2024, No. November-December, 21.10.2024, p. 5289-5298.

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@article{7659115a4d8c4147aa243bf9cbaa847b,
title = "Revealing the embrittlement phenomena after post-weld heat treatment of high-strength weld metal using high-resolution microscopy",
abstract = "High strength combined with sufficient toughness is a fundamental prerequisite for steel in the field of lightweight construction. Joining high-strength steels by means of welding requires the use of highly advanced filler metals and a stress-relief post-weld heat treatment (PWHT) for optimum performance of the joint. However, such a heat treatment can lead to embrittlement in the weld metal. In this context, the present work deals with the influence of different PWHT holding temperatures on the microstructure and mechanical properties of a high-strength multipass all-weld metal to reveal the embrittlement phenomena. The all-weld metal was fabricated via gas metal arc welding using a metal cored wire with a minimum yield strength of 690 MPa. Charpy V-notch impact testing and tensile testing were carried out to characterize the strength and toughness of the all-weld metal in the as-welded condition and after a 2 h stress-relief PWHT at 520 °C, 580 °C, and 620 °C. The microstructure was characterized utilizing high-resolution techniques such as atom probe tomography and high-energy X-ray diffraction. The strength and toughness of the all-weld metal both decrease after PWHT with different holding temperatures. The cause for the observed embrittlement was found to be the formation of Mn-rich cementite precipitates. These carbides increase in size and phase fraction with increasing holding temperature and lead to a brittle transcrystalline cleavage fracture. Consequently, it was concluded that a gas metal arc welded joint with the investigated filler metal should not be exposed to stress-relief PWHT at temperatures higher than 580 °C.",
author = "Daniel Schrittwieser and Hannes Pahr and Michael Musi and Andreas Landefeld and Oleksandr Glushko and Ronald Schnitzer",
year = "2024",
month = oct,
day = "21",
doi = "10.1016/j.jmrt.2024.10.186",
language = "English",
volume = "33.2024",
pages = "5289--5298",
journal = "Journal of Materials Research and Technology",
issn = "2238-7854",
publisher = "Elsevier",
number = "November-December",

}

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TY - JOUR

T1 - Revealing the embrittlement phenomena after post-weld heat treatment of high-strength weld metal using high-resolution microscopy

AU - Schrittwieser, Daniel

AU - Pahr, Hannes

AU - Musi, Michael

AU - Landefeld, Andreas

AU - Glushko, Oleksandr

AU - Schnitzer, Ronald

PY - 2024/10/21

Y1 - 2024/10/21

N2 - High strength combined with sufficient toughness is a fundamental prerequisite for steel in the field of lightweight construction. Joining high-strength steels by means of welding requires the use of highly advanced filler metals and a stress-relief post-weld heat treatment (PWHT) for optimum performance of the joint. However, such a heat treatment can lead to embrittlement in the weld metal. In this context, the present work deals with the influence of different PWHT holding temperatures on the microstructure and mechanical properties of a high-strength multipass all-weld metal to reveal the embrittlement phenomena. The all-weld metal was fabricated via gas metal arc welding using a metal cored wire with a minimum yield strength of 690 MPa. Charpy V-notch impact testing and tensile testing were carried out to characterize the strength and toughness of the all-weld metal in the as-welded condition and after a 2 h stress-relief PWHT at 520 °C, 580 °C, and 620 °C. The microstructure was characterized utilizing high-resolution techniques such as atom probe tomography and high-energy X-ray diffraction. The strength and toughness of the all-weld metal both decrease after PWHT with different holding temperatures. The cause for the observed embrittlement was found to be the formation of Mn-rich cementite precipitates. These carbides increase in size and phase fraction with increasing holding temperature and lead to a brittle transcrystalline cleavage fracture. Consequently, it was concluded that a gas metal arc welded joint with the investigated filler metal should not be exposed to stress-relief PWHT at temperatures higher than 580 °C.

AB - High strength combined with sufficient toughness is a fundamental prerequisite for steel in the field of lightweight construction. Joining high-strength steels by means of welding requires the use of highly advanced filler metals and a stress-relief post-weld heat treatment (PWHT) for optimum performance of the joint. However, such a heat treatment can lead to embrittlement in the weld metal. In this context, the present work deals with the influence of different PWHT holding temperatures on the microstructure and mechanical properties of a high-strength multipass all-weld metal to reveal the embrittlement phenomena. The all-weld metal was fabricated via gas metal arc welding using a metal cored wire with a minimum yield strength of 690 MPa. Charpy V-notch impact testing and tensile testing were carried out to characterize the strength and toughness of the all-weld metal in the as-welded condition and after a 2 h stress-relief PWHT at 520 °C, 580 °C, and 620 °C. The microstructure was characterized utilizing high-resolution techniques such as atom probe tomography and high-energy X-ray diffraction. The strength and toughness of the all-weld metal both decrease after PWHT with different holding temperatures. The cause for the observed embrittlement was found to be the formation of Mn-rich cementite precipitates. These carbides increase in size and phase fraction with increasing holding temperature and lead to a brittle transcrystalline cleavage fracture. Consequently, it was concluded that a gas metal arc welded joint with the investigated filler metal should not be exposed to stress-relief PWHT at temperatures higher than 580 °C.

U2 - 10.1016/j.jmrt.2024.10.186

DO - 10.1016/j.jmrt.2024.10.186

M3 - Article

VL - 33.2024

SP - 5289

EP - 5298

JO - Journal of Materials Research and Technology

JF - Journal of Materials Research and Technology

SN - 2238-7854

IS - November-December

ER -