Polypropylene Filled With Glass Spheres in Extrusion‐Based Additive Manufacturing: Effect of Filler Size and Printing Chamber Temperature

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@article{45eccda3be174697a3d9b651d734ac6c,
title = "Polypropylene Filled With Glass Spheres in Extrusion‐Based Additive Manufacturing: Effect of Filler Size and Printing Chamber Temperature",
abstract = "A challenge in extrusion‐based additive manufacturing of polypropylene (PP) filled with spherical particles is the combination of decent processability, excellent warpage control, and the retention of the tensile strength of neat PP. This study addresses this issue by adopting two approaches. Firstly, different size fractions of borosilicate glass spheres incorporated into PP are compared. Secondly, the temperature of the printing chamber (TCh) is varied. The effects of these features on the thermal, crystalline, morphological, tensile, impact, and warpage properties of 3D‐printed parts are examined. Smaller glass spheres (<12 µm) are found to be superior to larger fractions in all investigated aspects. Notably, the corresponding composites show higher tensile strengths than neat PP. An increase in TCh results in a more homogeneous temperature distribution within the printing chamber and promotes annealing during printing. Consequently, the dimensional accuracy of printed parts is improved. Additionally, β‐crystals and larger spherulites are formed at a higher TCh. ",
author = "Martin Sp{\"o}rk and Florian Arbeiter and Ivan Ragu{\v z} and Georg Weingrill and Thomas Fischinger and Gerhard Traxler and Stephan Schuschnigg and Ludwig Cardon and Clemens Holzer",
year = "2018",
month = may,
day = "16",
doi = "10.1002/mame.201800179",
language = "English",
volume = "303.2018",
journal = "Macromolecular materials and engineering",
issn = "1438-7492",
publisher = "Wiley-VCH ",
number = "7",

}

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TY - JOUR

T1 - Polypropylene Filled With Glass Spheres in Extrusion‐Based Additive Manufacturing

T2 - Effect of Filler Size and Printing Chamber Temperature

AU - Spörk, Martin

AU - Arbeiter, Florian

AU - Raguž, Ivan

AU - Weingrill, Georg

AU - Fischinger, Thomas

AU - Traxler, Gerhard

AU - Schuschnigg, Stephan

AU - Cardon, Ludwig

AU - Holzer, Clemens

PY - 2018/5/16

Y1 - 2018/5/16

N2 - A challenge in extrusion‐based additive manufacturing of polypropylene (PP) filled with spherical particles is the combination of decent processability, excellent warpage control, and the retention of the tensile strength of neat PP. This study addresses this issue by adopting two approaches. Firstly, different size fractions of borosilicate glass spheres incorporated into PP are compared. Secondly, the temperature of the printing chamber (TCh) is varied. The effects of these features on the thermal, crystalline, morphological, tensile, impact, and warpage properties of 3D‐printed parts are examined. Smaller glass spheres (<12 µm) are found to be superior to larger fractions in all investigated aspects. Notably, the corresponding composites show higher tensile strengths than neat PP. An increase in TCh results in a more homogeneous temperature distribution within the printing chamber and promotes annealing during printing. Consequently, the dimensional accuracy of printed parts is improved. Additionally, β‐crystals and larger spherulites are formed at a higher TCh.

AB - A challenge in extrusion‐based additive manufacturing of polypropylene (PP) filled with spherical particles is the combination of decent processability, excellent warpage control, and the retention of the tensile strength of neat PP. This study addresses this issue by adopting two approaches. Firstly, different size fractions of borosilicate glass spheres incorporated into PP are compared. Secondly, the temperature of the printing chamber (TCh) is varied. The effects of these features on the thermal, crystalline, morphological, tensile, impact, and warpage properties of 3D‐printed parts are examined. Smaller glass spheres (<12 µm) are found to be superior to larger fractions in all investigated aspects. Notably, the corresponding composites show higher tensile strengths than neat PP. An increase in TCh results in a more homogeneous temperature distribution within the printing chamber and promotes annealing during printing. Consequently, the dimensional accuracy of printed parts is improved. Additionally, β‐crystals and larger spherulites are formed at a higher TCh.

U2 - 10.1002/mame.201800179

DO - 10.1002/mame.201800179

M3 - Article

VL - 303.2018

JO - Macromolecular materials and engineering

JF - Macromolecular materials and engineering

SN - 1438-7492

IS - 7

M1 - 1800179

ER -