Impact of tensile specimen properties on hydrogen embrittlement testing using hollow specimens

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External Organisational units

  • voestalpine BÖHLER Edelstahl GmbH & Co KG

Abstract

This study investigates the influence of the bore-to-nominal diameter ratio ( d0/D0) on hydrogen embrittlement in a martensitic stainless-steel alloy through tensile testing of hollow specimens. Various geometries were tested, including one designed according to ISO 7039:2024 [1] standard. A conventional test at ambient pressure in air was used as a baseline for comparison. The primary aim was to assess how different d0/D0-ratios affect the mechanical properties and susceptibility to hydrogen embrittlement. In order to check the quality of the bore hole of the tensile tests, surface roughness measurements were conducted, as surface irregularities can significantly impact hydrogen-induced cracking.
The results indicate a strong correlation between the d0/D0 -ratio and the onset of hydrogen-induced fracture. Hollow specimens with higher d0/D0-ratios depicted premature failure compared to those with lower ratios. A comparison of fracture behavior between solid and hollow specimens, tested in inert and ambient atmospheres, highlighted significant differences in the fracture mechanisms. Notably, the yielding strengths and ultimate tensile
strength remained comparable and independent of the d0/D0-ratio and environment (Air, H2, and Ar). These findings suggest that a higher d0/D0 -ratio not only affects the stress distribution in tensile test specimens but also impacts the embrittlement process. The study offers a valuable contribution for optimizing the design of test specimens for hydrogen embrittlement testing.

References
[1] ISO 7039:2024, Metallic materials Tensile testing Method for evaluating the susceptibility of materials to the effects of high-pressure gas within hollow test pieces, 2024

Details

Translated title of the contributionEinfluss der Eigenschaften von Zugproben auf die Prüfung der Wasserstoffversprödung mittels Hohlproben
Original languageEnglish
Publication statusPublished - 12 Feb 2025
Event1st Conference on Hydrogen in Materials Science and Engineering - Rhein-Sieg-Forum, Siegburg/Bonn, Germany
Duration: 11 Feb 202513 Feb 2025
https://dgm.de/H2MSE/2025/

Conference

Conference1st Conference on Hydrogen in Materials Science and Engineering
Abbreviated titleH2MSE
Country/TerritoryGermany
CitySiegburg/Bonn
Period11/02/2513/02/25
Internet address