Dark-field X-ray microscopy reveals mosaicity and strain gradients across sub-surface TiC and TiN particles in steel matrix composites
Research output: Contribution to journal › Article › Research › peer-review
Authors
Organisational units
External Organisational units
- ESRF
- Technical University of Denmark
- Leti
- Materials Center Leoben Forschungs GmbH
Abstract
Residual strain gradients and crystallographic mosaicity across embedded ceramic particles within metal-matrix composites have remained experimentally inaccessible. In this work, we use synchrotron dark-field X-ray microscopy to characterize strain and orientation gradients across ~20 µm large TiC and TiN particles embedded in a steel matrix annealed at 480 and 600 °C. The results document gradual crystallographic orientation changes across the particles and the presence of sub-grains, in contrast to electron backscatter diffraction data. These gradients appear, however, not directly correlated with the observed strain gradients, which are attributed mainly to the different strain states within particles’ interiors and envelopes.
Details
Original language | English |
---|---|
Pages (from-to) | 402-406 |
Number of pages | 5 |
Journal | Scripta materialia |
Volume | 187.2020 |
Issue number | October |
DOIs | |
Publication status | Published - 2020 |