Binder System Composition on the Rheological and Magnetic Properties of Nd-Fe-B Feedstocks for Metal Injection Molding

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Binder System Composition on the Rheological and Magnetic Properties of Nd-Fe-B Feedstocks for Metal Injection Molding. / Momeni, Vahid; Luca, Sorana; Gonzalez-Gutierrez, Joamin et al.
In: Applied Sciences (Switzerland), Vol. 14.2024, No. 13, 5638, 07.2024.

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@article{f052dd946af8481a8676218dce0e50f5,
title = "Binder System Composition on the Rheological and Magnetic Properties of Nd-Fe-B Feedstocks for Metal Injection Molding",
abstract = "The applications of Nd-Fe-B-based magnets are experiencing significant diversification to achieve efficiency and miniaturization in different technologies. Metal injection molding (MIM) provides new opportunities to manufacture Nd-Fe-B magnets with high geometrical complexity efficiently. In this study, the impacts of the binder system composition and powder loading on the rheological behavior, contamination, and magnetic properties of the Nd-Fe-B MIM parts were investigated. A high-pressure capillary rheometer was used to measure the apparent viscosity and pressure drops for feedstocks with different binder formulations and powder contents. Also, oxygen and carbon contamination, density, and magnetic properties were measured for different feedstock formulations and powder loadings. From the rheological, density, and magnetic properties points of view, the binder system consisting of 45 vol.% LLDPE as backbone was selected as the optimum formulation. The findings indicated that the sample with this binder system and 55 vol.% powder content had a high density (6.83 g/cm3), remanence (0.591 T), and coercivity (744.6 kA/m) compared to other binder compositions. By using 58 vol.% powder loading, the values of density (7.54 g/cm3), remanence (0.618 T), and carbon residue (982 ppm) improved, and a suitable rheological behavior was still observed. Thus, a suitable feedstock formulation was developed.",
keywords = "binder system, carbon residue, magnetic properties, metal injection molding, rheological behavior",
author = "Vahid Momeni and Sorana Luca and Joamin Gonzalez-Gutierrez and Santiago Cano and Emilie Sueur and Zahra Shahroodi and Stephan Schuschnigg and Christian Kukla and Clemens Holzer",
note = "Publisher Copyright: {\textcopyright} 2024 by the authors.",
year = "2024",
month = jul,
doi = "10.3390/app14135638",
language = "English",
volume = "14.2024",
journal = "Applied Sciences (Switzerland)",
issn = "2076-3417",
publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",
number = "13",

}

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TY - JOUR

T1 - Binder System Composition on the Rheological and Magnetic Properties of Nd-Fe-B Feedstocks for Metal Injection Molding

AU - Momeni, Vahid

AU - Luca, Sorana

AU - Gonzalez-Gutierrez, Joamin

AU - Cano, Santiago

AU - Sueur, Emilie

AU - Shahroodi, Zahra

AU - Schuschnigg, Stephan

AU - Kukla, Christian

AU - Holzer, Clemens

N1 - Publisher Copyright: © 2024 by the authors.

PY - 2024/7

Y1 - 2024/7

N2 - The applications of Nd-Fe-B-based magnets are experiencing significant diversification to achieve efficiency and miniaturization in different technologies. Metal injection molding (MIM) provides new opportunities to manufacture Nd-Fe-B magnets with high geometrical complexity efficiently. In this study, the impacts of the binder system composition and powder loading on the rheological behavior, contamination, and magnetic properties of the Nd-Fe-B MIM parts were investigated. A high-pressure capillary rheometer was used to measure the apparent viscosity and pressure drops for feedstocks with different binder formulations and powder contents. Also, oxygen and carbon contamination, density, and magnetic properties were measured for different feedstock formulations and powder loadings. From the rheological, density, and magnetic properties points of view, the binder system consisting of 45 vol.% LLDPE as backbone was selected as the optimum formulation. The findings indicated that the sample with this binder system and 55 vol.% powder content had a high density (6.83 g/cm3), remanence (0.591 T), and coercivity (744.6 kA/m) compared to other binder compositions. By using 58 vol.% powder loading, the values of density (7.54 g/cm3), remanence (0.618 T), and carbon residue (982 ppm) improved, and a suitable rheological behavior was still observed. Thus, a suitable feedstock formulation was developed.

AB - The applications of Nd-Fe-B-based magnets are experiencing significant diversification to achieve efficiency and miniaturization in different technologies. Metal injection molding (MIM) provides new opportunities to manufacture Nd-Fe-B magnets with high geometrical complexity efficiently. In this study, the impacts of the binder system composition and powder loading on the rheological behavior, contamination, and magnetic properties of the Nd-Fe-B MIM parts were investigated. A high-pressure capillary rheometer was used to measure the apparent viscosity and pressure drops for feedstocks with different binder formulations and powder contents. Also, oxygen and carbon contamination, density, and magnetic properties were measured for different feedstock formulations and powder loadings. From the rheological, density, and magnetic properties points of view, the binder system consisting of 45 vol.% LLDPE as backbone was selected as the optimum formulation. The findings indicated that the sample with this binder system and 55 vol.% powder content had a high density (6.83 g/cm3), remanence (0.591 T), and coercivity (744.6 kA/m) compared to other binder compositions. By using 58 vol.% powder loading, the values of density (7.54 g/cm3), remanence (0.618 T), and carbon residue (982 ppm) improved, and a suitable rheological behavior was still observed. Thus, a suitable feedstock formulation was developed.

KW - binder system

KW - carbon residue

KW - magnetic properties

KW - metal injection molding

KW - rheological behavior

UR - http://www.scopus.com/inward/record.url?scp=85198462390&partnerID=8YFLogxK

U2 - 10.3390/app14135638

DO - 10.3390/app14135638

M3 - Article

AN - SCOPUS:85198462390

VL - 14.2024

JO - Applied Sciences (Switzerland)

JF - Applied Sciences (Switzerland)

SN - 2076-3417

IS - 13

M1 - 5638

ER -