TY - JOUR

T1 - The use of femtosecond laser ablation as a novel tool for rapid micro-mechanical sample preparation

AU - Pfeifenberger, Manuel J.

AU - Mangang, Melanie

AU - Wurster, Stefan

AU - Reiser, Jens

AU - Hohenwarter, Anton

AU - Pfleging, Wilhelm

AU - Kiener, Daniel

AU - Pippan, Reinhard

PY - 2017/5/5

Y1 - 2017/5/5

N2 - The focused ion beam technique has become a standard tool for micro-mechanical sample preparation in the last decade due to its high precision and general applicability in material removal. Besides disadvantages such as possible ion damage and high operation costs especially the characteristically small removal rates represent a bottleneck for this application. In contrast, femtosecond lasers provide material removal rates orders of magnitude higher, with small or ideally without thermal impact on the surrounding material. Hence, a combination of these two methods offers an ideal tool for time-efficient, micrometer-sized sample preparation. A prototype implementing this idea is presented here in combination with a case study. Cantilevers with a length of several hundred micrometers were machined into 25 μm, 50 μm and 100 μm thick, cold rolled tungsten foils. Scanning electron microscopy analyses reveal the influence of laser parameters and different scanning routines on the resulting sample quality and the effect of the laser pulse length (femtoseconds versus nanoseconds) on the ultra-fine grained microstructure. Finally, the performance for unprecedented rapid sample preparation is demonstrated with a sample array consisting of 100 cantilevers with a dimension of 420 ×60 ×25 μm3 processed in only half an hour, opening completely new testing possibilities.

AB - The focused ion beam technique has become a standard tool for micro-mechanical sample preparation in the last decade due to its high precision and general applicability in material removal. Besides disadvantages such as possible ion damage and high operation costs especially the characteristically small removal rates represent a bottleneck for this application. In contrast, femtosecond lasers provide material removal rates orders of magnitude higher, with small or ideally without thermal impact on the surrounding material. Hence, a combination of these two methods offers an ideal tool for time-efficient, micrometer-sized sample preparation. A prototype implementing this idea is presented here in combination with a case study. Cantilevers with a length of several hundred micrometers were machined into 25 μm, 50 μm and 100 μm thick, cold rolled tungsten foils. Scanning electron microscopy analyses reveal the influence of laser parameters and different scanning routines on the resulting sample quality and the effect of the laser pulse length (femtoseconds versus nanoseconds) on the ultra-fine grained microstructure. Finally, the performance for unprecedented rapid sample preparation is demonstrated with a sample array consisting of 100 cantilevers with a dimension of 420 ×60 ×25 μm3 processed in only half an hour, opening completely new testing possibilities.

KW - Femtosecond laser ablation

KW - Micro-mechanical testing

KW - Nanosecond laser ablation

KW - Sample preparation

KW - Ultra-fine grained tungsten

UR - http://www.scopus.com/inward/record.url?scp=85013757225&partnerID=8YFLogxK

U2 - 10.1016/j.matdes.2017.02.012

DO - 10.1016/j.matdes.2017.02.012

M3 - Article

AN - SCOPUS:85013757225

VL - 121.2017

SP - 109

EP - 118

JO - Materials and Design

JF - Materials and Design

SN - 0264-1275

IS - 5 May

ER -