MEMS-Based in situ electron-microscopy investigation of rapid solidification and heat treatment on eutectic Al-Cu
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In: Acta Materialia, Vol. 239.2022, No. 15 October, 118225, 15.10.2022.
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TY - JOUR
T1 - MEMS-Based in situ electron-microscopy investigation of rapid solidification and heat treatment on eutectic Al-Cu
AU - Dumitraschkewitz, Phillip
AU - Tunes, Matheus
AU - Quick, Cameron R.
AU - Santa Rosa Coradini, Diego
AU - Kremmer, Thomas
AU - Ramasamy, Parthiban
AU - Uggowitzer, Peter
AU - Pogatscher, Stefan
N1 - Publisher Copyright: © 2022 The Author(s)
PY - 2022/10/15
Y1 - 2022/10/15
N2 - The solidification behavior of a eutectic AlCu specimen is investigated via in situ scanning transmission electron microscope (STEM) experiments. Solidification conditions are varied by imposing various cooling conditions via a micro-electro-mechanical system (MEMS) based membrane. The methodology allows the use of material processed by a melting and casting route close to industrial metallurgically fabricated ma- terial for in situ STEM solidification studies. Different rapid solidification morphologies could be obtained solely on a single specimen by the demonstrated strategy. Additional post-solidification heat treatments are investigated in terms of observation of spheroidization of lamellas during annealing at elevated tem- peratures.
AB - The solidification behavior of a eutectic AlCu specimen is investigated via in situ scanning transmission electron microscope (STEM) experiments. Solidification conditions are varied by imposing various cooling conditions via a micro-electro-mechanical system (MEMS) based membrane. The methodology allows the use of material processed by a melting and casting route close to industrial metallurgically fabricated ma- terial for in situ STEM solidification studies. Different rapid solidification morphologies could be obtained solely on a single specimen by the demonstrated strategy. Additional post-solidification heat treatments are investigated in terms of observation of spheroidization of lamellas during annealing at elevated tem- peratures.
UR - http://www.scopus.com/inward/record.url?scp=85135848053&partnerID=8YFLogxK
U2 - 10.1016/j.actamat.2022.118225
DO - 10.1016/j.actamat.2022.118225
M3 - Article
VL - 239.2022
JO - Acta Materialia
JF - Acta Materialia
SN - 1359-6454
IS - 15 October
M1 - 118225
ER -