Data on production and characterization of melamine-furan-formaldehyde particles and reversible reactions thereof
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In: Data in Brief, Vol. 25.2019, No. August, 104056, 01.08.2019.
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TY - JOUR
T1 - Data on production and characterization of melamine-furan-formaldehyde particles and reversible reactions thereof
AU - Urdl, Katharina
AU - Weiss, Stephanie
AU - Hesser, Günter
AU - Kandelbauer, Andreas
AU - Zikulnig-Rusch, Edith
AU - Müller, Uwe
AU - Kern, Wolfgang
PY - 2019/8/1
Y1 - 2019/8/1
N2 - The data present in this article affords insides in the characterization of a newly described bi-functional furan-melamine monomer, which is used for the production of monodisperse, furan-functionalized melamine-formaldehyde particles, as described in https://doi.org/10.1016/j.eurpolymj.2019.04.006 Urdl et al., 2019. In the related research article Urdl et al., 2019 data interpretations can be found. The furan-functionalization of particles is necessary to perform reversible Diels-Alder reactions with maleimide (BMI) crosslinker to form thermoreversible network systems. To understand the reaction conditions of Diels-Alder (DA) reaction with a Fu-Mel monomer and a maleimide crosslinker, model DA reaction were performed and evaluated using dynamic FT-IR measurements. During retro Diels-Alder (rDA) reactions of the monomer system, it was found out that some side reaction occurred at elevated temperatures. The data of evaluating the side reaction is described in one part of this manuscript. Additional high resolution SEM images of Fu-Mel particles are shown and thermoreversible particle networks with BMI2 are shown. The data of different Fu-Mel particle networks with maleimide crosslinker are presented. Therefore, the used maleimide crosslinker with different spacer lengths were synthesized and the resulting networks were analyzed by ATR-FT-IR, SEM and DSC.
AB - The data present in this article affords insides in the characterization of a newly described bi-functional furan-melamine monomer, which is used for the production of monodisperse, furan-functionalized melamine-formaldehyde particles, as described in https://doi.org/10.1016/j.eurpolymj.2019.04.006 Urdl et al., 2019. In the related research article Urdl et al., 2019 data interpretations can be found. The furan-functionalization of particles is necessary to perform reversible Diels-Alder reactions with maleimide (BMI) crosslinker to form thermoreversible network systems. To understand the reaction conditions of Diels-Alder (DA) reaction with a Fu-Mel monomer and a maleimide crosslinker, model DA reaction were performed and evaluated using dynamic FT-IR measurements. During retro Diels-Alder (rDA) reactions of the monomer system, it was found out that some side reaction occurred at elevated temperatures. The data of evaluating the side reaction is described in one part of this manuscript. Additional high resolution SEM images of Fu-Mel particles are shown and thermoreversible particle networks with BMI2 are shown. The data of different Fu-Mel particle networks with maleimide crosslinker are presented. Therefore, the used maleimide crosslinker with different spacer lengths were synthesized and the resulting networks were analyzed by ATR-FT-IR, SEM and DSC.
KW - Diels-alder reaction
KW - Furan-functionalized particle
KW - Melamine-formaldehyde
KW - Thermoset
UR - http://www.scopus.com/inward/record.url?scp=85066743217&partnerID=8YFLogxK
U2 - 10.1016/j.dib.2019.104056
DO - 10.1016/j.dib.2019.104056
M3 - Article
AN - SCOPUS:85066743217
VL - 25.2019
JO - Data in Brief
JF - Data in Brief
SN - 2352-3409
IS - August
M1 - 104056
ER -