A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy

Publikationen: Beitrag in FachzeitschriftArtikelForschung(peer-reviewed)

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A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy. / Ebner, Anna Sophie; Brinckmann, Steffen; Plesiutschnig, Ernst et al.
in: JOM, Jahrgang 72.2020, Nr. 5, 16.03.2020, S. 2020-2029.

Publikationen: Beitrag in FachzeitschriftArtikelForschung(peer-reviewed)

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@article{597c4729ca1e48bc8756296b8cb591cd,
title = "A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy",
abstract = "An electrochemical charging setup was implemented in a nanoindentation system to evaluate the sensitivity of technically relevant materials to hydrogen embrittlement. Corresponding changes in the nanomechanical properties such as the hardness, Young{\textquoteright}s modulus and pop-in load can be measured and interpreted. A nickel-based alloy was examined in solution-annealed and aged condition. A hydrogen-induced hardness increase of 15% was measured for the solution-annealed sample. Aging the alloy leads to a reduced influence of hydrogen, lowering the hardness increase to 5%. For the solution-annealed sample, hydrogen charging-induced surface steps were observed and characterized with laser confocal microscopy and electron backscatter diffraction to reveal plastic deformation.",
author = "Ebner, {Anna Sophie} and Steffen Brinckmann and Ernst Plesiutschnig and Helmut Clemens and Reinhard Pippan and Verena Maier-Kiener",
year = "2020",
month = mar,
day = "16",
doi = "10.1007/s11837-020-04104-9",
language = "English",
volume = "72.2020",
pages = "2020--2029",
journal = "JOM",
issn = "0148-6608",
publisher = "Minerals, Metals and Materials Society",
number = "5",

}

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TY - JOUR

T1 - A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy

AU - Ebner, Anna Sophie

AU - Brinckmann, Steffen

AU - Plesiutschnig, Ernst

AU - Clemens, Helmut

AU - Pippan, Reinhard

AU - Maier-Kiener, Verena

PY - 2020/3/16

Y1 - 2020/3/16

N2 - An electrochemical charging setup was implemented in a nanoindentation system to evaluate the sensitivity of technically relevant materials to hydrogen embrittlement. Corresponding changes in the nanomechanical properties such as the hardness, Young’s modulus and pop-in load can be measured and interpreted. A nickel-based alloy was examined in solution-annealed and aged condition. A hydrogen-induced hardness increase of 15% was measured for the solution-annealed sample. Aging the alloy leads to a reduced influence of hydrogen, lowering the hardness increase to 5%. For the solution-annealed sample, hydrogen charging-induced surface steps were observed and characterized with laser confocal microscopy and electron backscatter diffraction to reveal plastic deformation.

AB - An electrochemical charging setup was implemented in a nanoindentation system to evaluate the sensitivity of technically relevant materials to hydrogen embrittlement. Corresponding changes in the nanomechanical properties such as the hardness, Young’s modulus and pop-in load can be measured and interpreted. A nickel-based alloy was examined in solution-annealed and aged condition. A hydrogen-induced hardness increase of 15% was measured for the solution-annealed sample. Aging the alloy leads to a reduced influence of hydrogen, lowering the hardness increase to 5%. For the solution-annealed sample, hydrogen charging-induced surface steps were observed and characterized with laser confocal microscopy and electron backscatter diffraction to reveal plastic deformation.

UR - http://www.scopus.com/inward/record.url?scp=85082742301&partnerID=8YFLogxK

U2 - 10.1007/s11837-020-04104-9

DO - 10.1007/s11837-020-04104-9

M3 - Article

VL - 72.2020

SP - 2020

EP - 2029

JO - JOM

JF - JOM

SN - 0148-6608

IS - 5

ER -